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**Metabolite-nulled macromolecules spectra measured at 3 T** Metabolite-nulled macromolecules spectra acquired from 10 healthy young volunteers scanned at 3 T using double-inversion recovery semi-LASER sequence with 8 echo times (20 - 62 ms) from two brain regions (prefrontal and occipital). Voxel-specific segmented brain values are included in Excel spreadsheet. More details about the acquisition can be found in the reference below. Format: **INSPECTOR** .mat, **jMRUI** .txt If you use this dataset, please cite this reference: Landheer K, Gajdošík M, Treacy M, Juchem C. **Concentration and effective T 2 relaxation times of macromolecules at 3T**. Magn Reson Med. 2020 Nov;84(5):2327-2337. doi: 10.1002/mrm.28282. Epub 2020 May 19. Pubmed: https://pubmed.ncbi.nlm.nih.gov/32430928/ INSPECTOR: http://innovation.columbia.edu/technologies/cu17130 jMRUI: http://www.jmrui.eu/
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